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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

5-Formyl-2H-pyrazole-3-carboxylic acid methyl ester synthesis

1synthesis methods
1H-Pyrazole-3-carboxylic acid, 5-(dimethoxymethyl)-, methyl ester

75436-38-3
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5-Formyl-2H-pyrazole-3-carboxylic acid methyl ester

75436-40-7
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Yield:75436-40-7 88%

Reaction Conditions:

with acetic acid at 60; for 1 h;

References:

Asano, Yasutomi;Kitamura, Shuji;Ohra, Taiichi;Itoh, Fumio;Kajino, Masahiro;Tamura, Tomoko;Kaneko, Manami;Ikeda, Shota;Igata, Hideki;Kawamoto, Tomohiro;Sogabe, Satoshi;Matsumoto, Shin-ichi;Tanaka, Toshimasa;Yamaguchi, Masashi;Kimura, Hiroyuki;Fukumoto, Shoji [Bioorganic and Medicinal Chemistry,2008,vol. 16,# 8,p. 4699 - 4714]