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ChemicalBook CAS DataBase List 8-METHOXY-2,3-DIHYDRO-1,4-BENZODIOXINE-6-CARBALDEHYDE

8-METHOXY-2,3-DIHYDRO-1,4-BENZODIOXINE-6-CARBALDEHYDE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hydroxide; copper / water / 27 h / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 100 - 105 °C

References:

Tsyganov, Dmitry V.;Konyushkin, Leonid D.;Karmanova, Irina B.;Firgang, Sergei I.;Strelenko, Yuri A.;Semenova, Marina N.;Kiselyov, Alex S.;Semenov, Victor V. [Journal of Natural Products,2013,vol. 76,# 8,p. 1485 - 1491]