2-Methyl-3-[(3,4-methylenedioxy)phenyl]propionic acid, 98% synthesis
- Product Name:2-Methyl-3-[(3,4-methylenedioxy)phenyl]propionic acid, 98%
- CAS Number:77269-66-0
- Molecular formula:C11H12O4
- Molecular Weight:208.21
1205-17-0
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$7.00/5g
77269-66-0
19 suppliers
$28.60/50MG
Yield:77269-66-0 84%
Reaction Conditions:
Stage #1: 3-(3,4-methylenedioxyphenyl)-2-methylpropan-1-alwith potassium peroxomonosulfate in N,N-dimethyl-formamide at 20 - 55; for 1 h;
Stage #2: with lithium hydroxide monohydrate in N,N-dimethyl-formamide;
References:
Schulze, Matthias [Synthetic Communications,2010,vol. 40,# 10,p. 1461 - 1476] Location in patent:experimental part