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ChemicalBook CAS DataBase List (S)-2-(tert-butoxycarbonylamino)-3-(pent-4-enyloxy)propanoic acid

(S)-2-(tert-butoxycarbonylamino)-3-(pent-4-enyloxy)propanoic acid synthesis

3synthesis methods
-

Yield:790305-00-9 76%

Reaction Conditions:

Stage #1: (S)-N-(tert-butoxycarbonyl)serinewith sodium hydride in water;N,N-dimethyl-formamide; for 0.5 h;Cooling with ice;
Stage #2: bromopentene in N,N-dimethyl-formamide at 20; for 16 h;

References:

Tang, Haoyu;Yin, Lichen;Lu, Hua;Cheng, Jianjun [Biomacromolecules,2012,vol. 13,# 9,p. 2609 - 2615]