Ethyl (1S,2R,3S,4S,5S)-2,3-O-(Isopropylidene)-4-hydroxybicyclo[3.1.0]hexanecarboxylate synthesis

7synthesis methods

Product Name:Ethyl (1S,2R,3S,4S,5S)-2,3-O-(Isopropylidene)-4-hydroxybicyclo[3.1.0]hexanecarboxylate
CAS Number:793695-59-7
Molecular formula:C12H18O5
Molecular Weight:242.27

Cyclopropa[3,4]cyclopenta[1,2-d]-1,3-dioxole-4a(3aH)-carboxylic acid, tetrahydro-5-hydroxy-2,2-dimethyl-, ethyl ester, (3aS,3bS,4aS,5R,5aR)-

828935-09-7
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Ethyl (1S,2R,3S,4S,5S)-2,3-O-(Isopropylidene)-4-hydroxybicyclo[3.1.0]hexanecarboxylate

793695-59-7
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$220.00/10mg

Yield:793695-59-7 55%

Reaction Conditions:

with trifluorormethanesulfonic acid in dichloromethane at 25; for 5 h;Inert atmosphere;

References:

Santhosh Kumar;Zhou, Si-Yuan;Joshi, Bhalchandra V.;Balasubramanian, Ramachandran;Yang, Tiehong;Liang, Bruce T.;Jacobson, Kenneth A. [Journal of Medicinal Chemistry,2010,vol. 53,# 6,p. 2562 - 2576] Location in patent:supporting information; experimental part

L-erythro-Pent-4-enose, 4,5-dideoxy-2,3-O-(1-methylethylidene)-

116669-78-4
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793695-59-7
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25581-41-3 Synthesis

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793695-59-7
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189996-60-9 Synthesis

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793695-59-7
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(4R,5S)-(2,2-DIMETHYL-5-VINYL-1,3-DIOXOLAN-4-YL)METHAN-1-OL

127758-25-2
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793695-59-7
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References