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7H-Benz[de]anthracen-7-one, 11-nitro- synthesis

4synthesis methods
93415-79-3 Synthesis
METHYL 2-IODO-3-NITROBENZOATE

93415-79-3
72 suppliers
$60.00/250mg

7H-Benz[de]anthracen-7-one, 11-nitro-

31536-41-1
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: Cu / dimethylformamide / 150 °C
2: aq. LiOH / methanol / 1 h / Heating
3: SOCl2
4: AlCl3 / CHCl3 / Ambient temperature

References:

Suzuki;Enya;Hisamatsu [Synthesis,1997,# 11,p. 1273 - 1276]