ChemicalBook CAS DataBase List 8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine

8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine synthesis

7synthesis methods

Product Name:8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine
CAS Number:50373-22-3
Molecular formula:C13H8Cl2N2
Molecular Weight:263.12

8-Chloro-5,10-dihydrodibenzo[b,e][1,4]diazepin-11-one

50892-62-1
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8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine

50373-22-3
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Yield:50373-22-3 72%

Reaction Conditions:

Stage #1: 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-onewith N,N-dimethyl-aniline;trichlorophosphate in toluene at 95; for 2 h;
Stage #2: with sodium carbonate in 1,4-dioxane at 80; for 1 h;

References:

Ottesen, Lars K.;Ek, Fredrik;Olsson, Roger [Organic Letters,2006,vol. 8,# 9,p. 1771 - 1773]

67990-66-3 Synthesis

N-(2-AMINO-4-CHLOROPHENYL)ANTHRANILIC ACID

67990-66-3
59 suppliers
$38.00/250mg

50373-22-3
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References

60091-87-4 Synthesis

2-[(4-CHLORO-2-NITROPHENYL)AMINO]-BENZOIC ACID

60091-87-4
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50373-22-3
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References

118-92-3
4 suppliers
$25.89/25g

50373-22-3
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References

345-18-6 Synthesis

345-18-6
196 suppliers
$7.00/5g

50373-22-3
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References

8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine Related Search:

2-AMINO-4-CHLORODIPHENYLAMINE