ChemicalBook CAS DataBase List (8α,9S)-9-aMino-Cinchonan-6'-ol

(8α,9S)-9-aMino-Cinchonan-6'-ol synthesis

3synthesis methods

Product Name:(8α,9S)-9-aMino-Cinchonan-6'-ol
CAS Number:960050-59-3
Molecular formula:C19H23N3O
Molecular Weight:309.41

130-95-0 Synthesis

130-95-0
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960050-59-3
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$83.00/50mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 4 h / 0 - 4 °C / Inert atmosphere
2: sodium azide / N,N-dimethyl-formamide / 16 h / 65 °C / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 - 4 °C / Inert atmosphere
4: sodium thioethylate / dimethyl sulfoxide / 72 h / 80 °C / Inert atmosphere

References:

EP2687527,2014,A1

Cinchonan-9-ol, 6'-methoxy-, 9-methanesulfonate, (8α,9R)-

249731-47-3
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960050-59-3
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References

Cinchonan, 9-azido-6'-methoxy-, (8α,9S)-

168778-61-8
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960050-59-3
14 suppliers
$83.00/50mg

References

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