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ChemicalBook CAS DataBase List 8-Amino-7-quinolinecarbaldehyde

8-Amino-7-quinolinecarbaldehyde synthesis

6synthesis methods
7471-63-8 Synthesis
7-METHYL-8-NITROQUINOLINE

7471-63-8
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$33.72/1g

8-Amino-7-quinolinecarbaldehyde

158753-17-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 99 percent / dimethylformamide / 16 h / 140 °C
2: 88 percent / sodium periodate / tetrahydrofuran; H2O / 2 h / 25 °C
3: 84 percent / Fe powder, conc. HCl / ethanol; acetic acid; H2O / 1) reflux, 15 min; 2) 25 deg C, 25 min

References:

Riesgo, Elvira C.;Jin, Xiaoqing;Thummel, Randolph P. [Journal of Organic Chemistry,1996,vol. 61,# 9,p. 3017 - 3022]