8-BroMo-1H-quinolin-4-one synthesis
- Product Name:8-BroMo-1H-quinolin-4-one
- CAS Number:949507-29-3
- Molecular formula:C9H6BrNO
- Molecular Weight:224.05
2033-24-1
635 suppliers
$6.00/25g
615-36-1
407 suppliers
$10.00/5g
949507-29-3
18 suppliers
$60.00/50mg
Yield:949507-29-3 88.4%
Reaction Conditions:
Stage #1: cycl-isopropylidene malonatewith trimethyl orthoformate for 4 h;Reflux;
Stage #2: 2-bromoaniline for 20 h;Resolution of racemate;
Stage #3: with diphenylether for 4 h;Reflux;
References:
Todorov, Aleksandar R.;Wirtanen, Tom;Helaja, Juho [Journal of Organic Chemistry,2017,vol. 82,# 24,p. 13756 - 13767]