ChemicalBook CAS DataBase List 8-Bromo-6-chloro-7H-purin-2-amine

8-Bromo-6-chloro-7H-purin-2-amine synthesis

2synthesis methods

Product Name:8-Bromo-6-chloro-7H-purin-2-amine
CAS Number:1262120-94-4
Molecular formula:C5H3BrClN5
Molecular Weight:248.47

9H-Purin-2-amine, 6-chloro-N,9-bis(tetrahydro-2H-pyran-2-yl)-

171825-50-6
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1262120-94-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 2 h / -78 °C / Inert atmosphere
2.1: hydrogenchloride / water; ethylene glycol / 0.5 h / 20 °C

References:

Mahajan, Tushar R.;Ytre-Arne, Mari Eknes;Str?m-Andersen, Pernille;Dalhus, Bj?rn;Gundersen, Lise-Lotte [Molecules,2015,vol. 20,# 9,p. 15944 - 15965]

10310-21-1
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1262120-94-4
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References