8-hydrazinylquinoline hydrochloride synthesis
- Product Name:8-hydrazinylquinoline hydrochloride
- CAS Number:14148-42-6
- Molecular formula:C9H9N3
- Molecular Weight:159.19
Yield:14148-42-6 210 mg
Reaction Conditions:
Stage #1: 8-bromoquinoline;benzophenone hydrazonewith palladium diacetate;2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;sodium t-butanolate in toluene at 90; for 6 h;Inert atmosphere;
Stage #2: with hydrogenchloride;water in toluene at 90; for 19 h;Inert atmosphere;
References:
Xu, Yan;Young, Michael C.;Dong, Guangbin [Journal of the American Chemical Society,2017,vol. 139,# 16,p. 5716 - 5719] Location in patent:supporting information
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