1-Propanone, 3-[(4-methoxyphenyl)amino]-1,3-diphenyl- synthesis
- Product Name:1-Propanone, 3-[(4-methoxyphenyl)amino]-1,3-diphenyl-
- CAS Number:802-49-3
- Molecular formula:C22H21NO2
- Molecular Weight:331.41
Yield:802-49-3 131.1 mg
Reaction Conditions:
Stage #1: acetophenonewith diphenylsilane;chloro(1,5-cyclooctadiene)rhodium(I) dimer in dichloromethane at 20; for 6 h;
Stage #2: 4-methoxy-N-[(1Z)-phenylmethylene]aniline;ytterbium(III) triflate in dichloromethane at -23; for 1 h;
References:
Thiot, Carine;Wagner, Alain;Mioskowski, Charles [Organic Letters,2006,vol. 8,# 26,p. 5939 - 5942]
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