ChemicalBook CAS DataBase List 4-Pyridinecarboxylic acid, 3-(hydroxymethyl)- (9CI)

4-Pyridinecarboxylic acid, 3-(hydroxymethyl)- (9CI) synthesis

2synthesis methods

Product Name:4-Pyridinecarboxylic acid, 3-(hydroxymethyl)- (9CI)
CAS Number:81113-13-5
Molecular formula:C7H7NO3
Molecular Weight:153.14

3,4-Pyridinedicarboxylic acid dimethyl ester

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4-Pyridinecarboxylic acid, 3-(hydroxymethyl)- (9CI)

81113-13-5
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 5.3 g / sodium hydroxide, water / 1.5 h / 20 °C
2: 4.9 g / lithium aluminium hydride / tetrahydrofuran / 0.1 h / 0 - 2 °C

References:

Ashcroft, William R.;Beal, Michael G.;Joule, John A. [Journal of the Chemical Society. Perkin transactions I,1981,p. 3012 - 3015]

24202-79-7 Synthesis

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References