L-Norleucine, 6-bromo-N-[(1,1-dimethylethoxy)carbonyl]-, methyl ester synthesis

4synthesis methods

Product Name:L-Norleucine, 6-bromo-N-[(1,1-dimethylethoxy)carbonyl]-, methyl ester
CAS Number:81505-59-1
Molecular formula:C12H22BrNO4
Molecular Weight:324.21

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L-Norleucine, 6-bromo-N-[(1,1-dimethylethoxy)carbonyl]-, methyl ester

81505-59-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: Et₃N / tetrahydrofuran; H₂O / Ambient temperature
2: 90 percent / CH₂Cl₂ / 20 h / Heating
3: CBr₄, PPh₃ / tetrahydrofuran / Ambient temperature

References:

Maurer, Peter J.;Miller, Marvin J. [Journal of the American Chemical Society,1982,vol. 104,# 11,p. 3096 - 3101]

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References

24424-99-5 Synthesis

24424-99-5
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References

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References