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10-nitro-2,6-dioxabicyclo[5.4.0]undeca-8,10,12-trien-9-amine synthesis

1synthesis methods
2H-1,5-Benzodioxepin, 3,4-dihydro-7,8-dinitro-

135399-50-7
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Yield:81864-62-2 48%

Reaction Conditions:

with ammonium hydroxide in ethanol at 123 - 134; for 3 h;

References:

Hadjimihalakis, Phaedon M. [Journal of Heterocyclic Chemistry,1991,vol. 28,# 4,p. 1111 - 1114]

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