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ChemicalBook CAS DataBase List 4,8-Dioxa-3,9-disilaundecane, 2,2,3,3,9,9,10,10-octamethyl-

4,8-Dioxa-3,9-disilaundecane, 2,2,3,3,9,9,10,10-octamethyl- synthesis

3synthesis methods
77377-52-7 Synthesis
N-(tert-Butyldimethylsilyl)-N-methyl-trifluoroacetamide

77377-52-7
162 suppliers
$24.00/1g

504-63-2 Synthesis
1,3-Propanediol

504-63-2
531 suppliers
$9.00/5g

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Yield:82112-22-9 100%

Reaction Conditions:

with tert-butyldimethylsilyl chloride in acetonitrile; for 0.0833333 h;Product distribution;Ambient temperature;other tert-butyldimethylsilyl- donors; other alkohols; other solvent, temp. and time;

References:

Mawhinney, Thomas P.;Madson, Michael A. [Journal of Organic Chemistry,1982,vol. 47,# 17,p. 3336 - 3339]

18162-48-6 Synthesis
tert-Butyldimethylsilyl chloride

18162-48-6
665 suppliers
$9.00/5g

504-63-2 Synthesis
1,3-Propanediol

504-63-2
531 suppliers
$9.00/5g

73842-99-6 Synthesis
3-(T-BUTYLDIMETHYLSILOXY)PROPANOL

73842-99-6
125 suppliers
$6.00/1g