ChemicalBook CAS DataBase List 6,7-DIHYDRO-2-PHENYL-5H-PYRROLO[2,1-C]-1,2,4-TRIAZOLIUM CHLORIDE

6,7-DIHYDRO-2-PHENYL-5H-PYRROLO[2,1-C]-1,2,4-TRIAZOLIUM CHLORIDE synthesis

2synthesis methods

Product Name:6,7-DIHYDRO-2-PHENYL-5H-PYRROLO[2,1-C]-1,2,4-TRIAZOLIUM CHLORIDE
CAS Number:828914-68-7
Molecular formula:C11H12ClN3
Molecular Weight:221.69

616-45-5 Synthesis

616-45-5
373 suppliers
$14.00/5g

100-63-0 Synthesis

100-63-0
359 suppliers
$10.00/1g

77-78-1
290 suppliers
$19.69/1ml

149-73-5 Synthesis

149-73-5
521 suppliers
$12.00/5g

6,7-DIHYDRO-2-PHENYL-5H-PYRROLO[2,1-C]-1,2,4-TRIAZOLIUM CHLORIDE

828914-68-7
38 suppliers
$70.00/100mg

Yield: 72%

Reaction Conditions:

Stage #1:2-pyrrolidinon;dimethyl sulfate in acetonitrile at 80; for 17 h;
Stage #2:phenylhydrazine in acetonitrile at 80; for 4 h;
Stage #3:trimethyl orthoformateFurther stages;

References:

Kena-diba, Anastasie;Noll, Claudia;Richter, Michael;Gieseler, Marc Timo;Kalesse, Markus [Angewandte Chemie - International Edition,2010,vol. 49,# 45,p. 8367 - 8369] Location in patent:supporting information; experimental part

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
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149-73-5 Synthesis

149-73-5
521 suppliers
$12.00/5g

828914-68-7
38 suppliers
$70.00/100mg

References