5-PyriMidinecarboxylic acid, 4-[1,1'-biphenyl]-4-yl-1-[6-[[2-(butylaMino)-1-[3-(Methoxycarbonyl)-4-(2-Methoxy-2-oxoethoxy)phenyl]-2-oxoethyl]hexylaMino]-6-oxohexyl]-1,2,3,4-tetrahydro-6-Methyl-2-oxo-, phenylMethyl ester synthesis

3synthesis methods

Product Name:5-PyriMidinecarboxylic acid, 4-[1,1'-biphenyl]-4-yl-1-[6-[[2-(butylaMino)-1-[3-(Methoxycarbonyl)-4-(2-Methoxy-2-oxoethoxy)phenyl]-2-oxoethyl]hexylaMino]-6-oxohexyl]-1,2,3,4-tetrahydro-6-Methyl-2-oxo-, phenylMethyl ester
CAS Number:831217-40-4
Molecular formula:C54H66N4O10
Molecular Weight:931.1226

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 76 percent / HCl / tetrahydrofuran / 96 h / 20 °C
2: 19 percent / methanol / 24 h / Heating

References:

Werner, Stefan;Turner, David M.;Lyon, Michael A.;Huryn, Donna M.;Wipf, Peter [Synlett,2006,# 14,p. 2334 - 2338]