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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

1-METHYLSPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDIN]-2(1H)-ONE synthesis

4synthesis methods
Spiro[4H-3,1-benzoxazine-4,4'-piperidine]-1'-carboxylic acid, 1,2-dihydro-1-methyl-2-oxo-, 1,1-dimethylethyl ester

345938-03-6
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1-METHYLSPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDIN]-2(1H)-ONE

84060-10-6
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Yield:84060-10-6 78%

Reaction Conditions:

with trifluoroacetic acid in dichloromethane; for 2 h;Ambient temperature;

References:

Clark;Caroon;Kluge;Repke;Roszkowski;Strosberg;Baker;Bitter;Okada [Journal of Medicinal Chemistry,1983,vol. 26,# 5,p. 657 - 661]

3422-01-3 Synthesis
N-BOC ANILINE

3422-01-3
93 suppliers
$10.00/1g

1-METHYLSPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDIN]-2(1H)-ONE

84060-10-6
10 suppliers
inquiry

References
79099-07-3 Synthesis
N-(tert-Butoxycarbonyl)-4-piperidone

79099-07-3
543 suppliers
$5.00/5g

1-METHYLSPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDIN]-2(1H)-ONE

84060-10-6
10 suppliers
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References
1,2-DIHYDRO-2-OXO-SPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDINE]-1'-CARBOXYLIC ACID 1,1-DIMETHYL ETHYL ESTER

84060-08-2
41 suppliers
$51.00/100mg

1-METHYLSPIRO[4H-3,1-BENZOXAZINE-4,4'-PIPERIDIN]-2(1H)-ONE

84060-10-6
10 suppliers
inquiry

References