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ChemicalBook CAS DataBase List α-D-galactopyranoside,methy-4-deoxy-4-fluoro-,tribenzoate

α-D-galactopyranoside,methy-4-deoxy-4-fluoro-,tribenzoate synthesis

3synthesis methods
-

Yield:84065-98-5 79.4%

Reaction Conditions:

with (bis-(2-methoxyethyl)amino)sulfur trufluoride in tetrahydrofuran at 20 - 52;Large scale reaction;

References:

Weiberth, Franz J.;Gill, Harpal S.;Jiang, Ying;Lee, George E.;Lienard, Philippe;Pemberton, Clive;Powers, Matthew R.;Subotkowski, Witold;Tomasik, Witold;Vanasse, Benoit J.;Yu, Yong [Organic Process Research and Development,2010,vol. 14,# 3,p. 623 - 631] Location in patent:experimental part