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Carbamic acid, N-(3-iodopropyl)-, phenylmethyl ester synthesis

4synthesis methods
2304-94-1 Synthesis
Carbobenzyloxy-beta-alanine

2304-94-1
221 suppliers
$5.00/1g

Carbamic acid, N-(3-iodopropyl)-, phenylmethyl ester

84792-78-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran / 0.25 h / -15 °C
1.2: 0.5 h
1.3: 0.25 h
2.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 6 h

References:

Santhosh;Durgamma;Shekharappa;Sureshbabu, Vommina V. [Organic and Biomolecular Chemistry,2018,vol. 16,# 26,p. 4874 - 4880]