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ChemicalBook CAS DataBase List (S)-(-)-ALPHA,ALPHA-DIPHENYL-2-PYRROLIDINYL METHYLTMS ETHER
848821-58-9

(S)-(-)-ALPHA,ALPHA-DIPHENYL-2-PYRROLIDINYL METHYLTMS ETHER synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: potassium carbonate / 7.5 h / 0 - 20 °C / Inert atmosphere
2.1: tetrahydrofuran / 20 °C / Inert atmosphere
2.2: 16 h / Reflux; Inert atmosphere
3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

References:

Khong, San N.;Kwon, Ohyun [Molecules,2012,vol. 17,# 5,p. 5626 - 5650]

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