BROMO[(2-(HYDROXY-KAPPAO)METHYL)PHENYLMETHYL-KAPPAC](TRIPHENYLPHOSPHINE)PALLADIUM(II) synthesis
- Product Name:BROMO[(2-(HYDROXY-KAPPAO)METHYL)PHENYLMETHYL-KAPPAC](TRIPHENYLPHOSPHINE)PALLADIUM(II)
- CAS Number:849417-33-0
- Molecular formula:C18H15P.C8H9BrOPd
- Molecular Weight:569.773
14221-01-3
600 suppliers
$22.00/1g
74785-02-7
42 suppliers
$35.00/100mg
849417-33-0
14 suppliers
$457.00/1g
Yield:849417-33-0 86%
Reaction Conditions:
in toluene;(N2); Schlenk technique; soln. of ligand (1 equiv.) in toluene was addeddropwise to stirred suspn. of Pd complex (1 equiv.) in toluene; mixt. w as stirred at room temp. for 12 h; filtered; washed (Et2O); dried (vac.); crystd. (CH2Cl2/petroleum ether);elem. anal.;
References:
Lindsell, W. Edward;Palmer, Daniel D.;Preston, Peter N.;Rosair, Georgina M.;Jones, Ray V. H.;Whitton, Alan J. [Organometallics,2005,vol. 24,# 6,p. 1119 - 1133]