4-[3-(1,3-BENZODIOXOL-5-YL)-1,2,4-OXADIAZOL-5-YL]PIPERIDINE synthesis
- Product Name:4-[3-(1,3-BENZODIOXOL-5-YL)-1,2,4-OXADIAZOL-5-YL]PIPERIDINE
- CAS Number:849925-04-8
- Molecular formula:C14H15N3O3
- Molecular Weight:273.29
4421-09-4
153 suppliers
$8.00/1g
849925-04-8
15 suppliers
$120.00/1g
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol; water / 12 h / Reflux
2.1: 1,1'-carbonyldiimidazole / acetonitrile / 1 h / 20 °C
2.2: 12 h / 20 °C
3.1: N,N-dimethyl-formamide / 3 h / 120 - 125 °C
References:
Konyushkin;Godovikova;Vorontsova;Tsyganov;Karmanova;Raihstat;Firgang;Pokrovskii;Pokrovskii;Semenova;Semenov [Russian Chemical Bulletin,2010,vol. 59,# 12,p. 2268 - 2275]
4720-72-3
40 suppliers
$45.00/100mg
849925-04-8
15 suppliers
$120.00/1g