ChemicalBook CAS DataBase List 3,3'-dihydroxy-[1,1'-biphenyl]-4,4'-dicarboxylic acid

3,3'-dihydroxy-[1,1'-biphenyl]-4,4'-dicarboxylic acid synthesis

12synthesis methods

Product Name:3,3'-dihydroxy-[1,1'-biphenyl]-4,4'-dicarboxylic acid
CAS Number:861533-46-2
Molecular formula:C14H10O6
Molecular Weight:274.23

22717-56-2 Synthesis

22717-56-2
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3,3'-dihydroxy-[1,1'-biphenyl]-4,4'-dicarboxylic acid

861533-46-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium carbonate / acetonitrile / 75 °C
2.1: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; cesium fluoride / 1,4-dioxane; water / 85 °C
3.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; methanol / 50 °C
3.2: 85 °C

References:

Feng, Liang;Li, Jia-Luo;Day, Gregory S.;Lv, Xiu-Liang;Zhou, Hong-Cai [Chem,2019,vol. 5,# 5,p. 1265 - 1274]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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861533-46-2
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References

[1,1'-Biphenyl]-4,4'-dicarboxylic acid, 3,3'-dihydroxy-, 4,4'-dimethyl ester

148490-98-6
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861533-46-2
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References

18179-39-0
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861533-46-2
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References

854028-46-9
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861533-46-2
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References