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4-Acetyl-3,4-dihydro-2H-benzo[1,4]oxazine-3-carbonitrile synthesis

2synthesis methods
7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
373 suppliers
$19.00/5g

Ethanone, 1-(2,3-dihydro-3-methoxy-4H-1,4-benzoxazin-4-yl)-

86267-82-5
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4-Acetyl-3,4-dihydro-2H-benzo[1,4]oxazine-3-carbonitrile

86267-88-1
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Yield:86267-88-1 96%

Reaction Conditions:

with boron trifluoride in diethyl ether; for 24 h;Ambient temperature;

References:

Bartsch, Herbert;Schwarz, Otto [Journal of Heterocyclic Chemistry,1983,vol. 20,p. 45 - 48]