(alphaS)-alpha-Aminobenzenebutanoyl-L-leucyl-L-phenylalanine methyl ester mono(trifluoroacetate) synthesis
- Product Name:(alphaS)-alpha-Aminobenzenebutanoyl-L-leucyl-L-phenylalanine methyl ester mono(trifluoroacetate)
- CAS Number:868539-99-5
- Molecular formula:C28H36F3N3O5
- Molecular Weight:551.5978
2577-90-4
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
2: dichloromethane / 3 h / 0 - 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
4: dichloromethane / 3 h / 0 - 20 °C
References:
Lei, Meng;Zhang, Haoyang;Miao, Hang;Du, Xiao;Zhou, Hui;Wang, Jia;Wang, Xueyuan;Feng, Huayun;Shi, Jingmiao;Liu, Zhaogang;Shen, Jian;Zhu, Yongqiang [Bioorganic and Medicinal Chemistry,2019,vol. 27,# 18,p. 4151 - 4162]
13734-34-4
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