ChemicalBook CAS DataBase List 2,8-Dibromo-6,6,12,12-tetrahexyl-6,12-dihydroindeno[1,2-b]fluorene

2,8-Dibromo-6,6,12,12-tetrahexyl-6,12-dihydroindeno[1,2-b]fluorene synthesis

1synthesis methods

Product Name:2,8-Dibromo-6,6,12,12-tetrahexyl-6,12-dihydroindeno[1,2-b]fluorene
CAS Number:872705-69-6
Molecular formula:C44H60Br2
Molecular Weight:748.76

Indeno[1,2-b]fluorene, 6,6,12,12-tetrahexyl-6,12-dihydro-

872705-68-5
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2,8-Dibromo-6,6,12,12-tetrahexyl-6,12-dihydroindeno[1,2-b]fluorene

872705-69-6
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Yield:872705-69-6 73%

Reaction Conditions:

with benzyltrimethylazanium tribroman-2-uide;zinc(II) chloride in acetic acid at 70; for 12 h;Inert atmosphere;

References:

Lin, Tzu-Chau;Hsu, Cheng-Sheng;Hu, Chia-Ling;Chen, Yong-Fu;Huang, Wei-Je [Tetrahedron Letters,2009,vol. 50,# 2,p. 182 - 185] Location in patent:supporting information; experimental part