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ChemicalBook CAS DataBase List 4-[3-(TrifluoroMethyl)-3H-diazirin-3-yl]benzyl Alcohol

4-[3-(TrifluoroMethyl)-3H-diazirin-3-yl]benzyl Alcohol synthesis

14synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 95 percent / cyanuric fluoride, pyridine / CH2Cl2 / 2 h / -20 - -10 °C
2: 84 percent / LiBH4 / tetrahydrofuran; methanol / 1 h / Ambient temperature

References:

Latli, Bachir;Morimoto, Hiromi;Williams, Philip G.;Casida, John E. [Journal of labelled compounds and radiopharmaceuticals,1998,vol. 41,# 3,p. 191 - 199]