ChemicalBook CAS DataBase List 3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97%

3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97% synthesis

7synthesis methods

Product Name:3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97%
CAS Number:883738-27-0
Molecular formula:C18H29BN2O2
Molecular Weight:316.25

109-01-3 Synthesis

109-01-3
646 suppliers
$5.00/5G

443776-76-9 Synthesis

(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

443776-76-9
101 suppliers
$8.00/250mg

3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97%

883738-27-0
71 suppliers
$10.00/100mg

Yield:883738-27-0 80%

Reaction Conditions:

with [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂;sodium carbonate;bis[2-(diphenylphosphino)phenyl] ether in 5,5-dimethyl-1,3-cyclohexadiene at 155; for 24 h;Inert atmosphere;Reflux;

References:

Ma, Winson M. J.;James, Tony D.;Williams, Jonathan M. J. [Organic Letters,2013,vol. 15,# 18,p. 4850 - 4853] Location in patent:supporting information

331977-03-8 Synthesis