ChemicalBook CAS DataBase List 3-Methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenol

3-Methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenol synthesis

2synthesis methods

Product Name:3-Methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenol
CAS Number:889659-70-5
Molecular formula:C13H19BO3
Molecular Weight:234.1

Methanesulfonic acid, 1,1,1-trifluoro-, 3-hydroxy-5-methylphenyl ester

889659-69-2
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73183-34-3
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3-Methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenol

889659-70-5
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$45.00/25mg

Yield:889659-70-5 84%

Reaction Conditions:

with methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II);potassium acetate in 1,4-dioxane;toluene at 95; for 16 h;Inert atmosphere;

References:

Neel, Andrew J.;Milo, Anat;Sigman, Matthew S.;Toste, F. Dean [Journal of the American Chemical Society,2016,vol. 138,# 11,p. 3863 - 3875] Location in patent:supporting information

504-15-4 Synthesis

504-15-4
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889659-70-5
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$45.00/25mg

References