ChemicalBook CAS DataBase List (S)-3-BENZYLOXYCARBONYL-4-(3-OXOBUTYL)-5-OXAZILIDINONE

(S)-3-BENZYLOXYCARBONYL-4-(3-OXOBUTYL)-5-OXAZILIDINONE synthesis

3synthesis methods

Product Name:(S)-3-BENZYLOXYCARBONYL-4-(3-OXOBUTYL)-5-OXAZILIDINONE
CAS Number:89662-51-1
Molecular formula:C15H17NO5
Molecular Weight:291.3

(S)-(+)-3-(BENZYLOXYCARBONYL)-5-OXO-4-OXAZOLIDINEPROPIONIC ACID

23632-67-9
48 suppliers
$73.79/1g

(S)-3-BENZYLOXYCARBONYL-4-(3-OXOBUTYL)-5-OXAZILIDINONE

89662-51-1
15 suppliers
$90.00/25mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: N-methylmorpholine / tetrahydrofuran / 0.5 h / -15 °C
2: Et₃N / tetrahydrofuran / 1 h / -15 °C
3: iodoform / 1,1,1-trichloro-ethane / 3 h / Irradiation
4: 1.) Zn, Cu / 2.) Pd(PPh₃)2Cl₂ / 1.) DMA, benzene, irradiation, 30 min, 2.) DMA, benzene, 25-35 deg C, 1 h

References:

Jackson, Richard F. W.;Fraser, Joanne L.;Wishart, Neil;Porter, Barry;Wythes, Martin J. [Journal of the Chemical Society. Perkin transactions I,1998,# 12,p. 1903 - 1912]

(S)-benzyl 4-(3-chloro-3-oxopropyl)-5-
oxooxazolidine-3-carboxylate

58456-26-1
2 suppliers
inquiry

89662-51-1
15 suppliers
$90.00/25mg

References

1155-62-0
354 suppliers
$10.00/5g

89662-51-1
15 suppliers
$90.00/25mg

References