ChemicalBook CAS DataBase List 5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE

5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE synthesis

5synthesis methods

Product Name:5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE
CAS Number:89809-89-2
Molecular formula:C15H14N2O2
Molecular Weight:254.28

100-52-7 Synthesis

100-52-7
942 suppliers
$21.30/2g

105-45-3
649 suppliers
$5.00/5g

109-77-3 Synthesis

109-77-3
425 suppliers
$10.00/5g

5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE

89809-89-2
20 suppliers
$30.00/20mg

Yield:89809-89-2 96%

Reaction Conditions:

with Ferric Sulfasalazine Sulfa Drug Complex Supported on Cobalt Ferrite Cellulose in ethanol at 60; for 0.15 h;

Steps:

2.3 General Procedure for the 4H- Pyrans Derivatives Synthesis

General procedure: A suspension of malonitrile (1mmol), ethyl acetoacetate(methyl acetoacetate, acetoacetate) (1mmol), aldehyde(1mmol) and the catalyst (0.01g, 0.0016mmol) in ethanol(10ml) was stirred at 60°C. After completion of the reactionwhich was monitored by TLC, the catalyst was separatedby using an external magnet. The mixture was poured into cold water and the precipitate was filtered. The solid wasrecrystallized with ethanol and dried in an oven at 60°C.

References:

Rostamizadeh, Shahnaz;Daneshfar, Zahra;Khazaei, Ali [Catalysis Letters,2020,vol. 150,# 7,p. 2091 - 2114]

100-52-7 Synthesis

100-52-7
942 suppliers
$21.30/2g

123-54-6 Synthesis