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9-AMino(9-deoxy)epi-diquinidine trihydrochloride synthesis
- Product Name:9-AMino(9-deoxy)epi-diquinidine trihydrochloride
- CAS Number:522600-31-3
- Molecular formula:C20H27N3O
- Molecular Weight:325.45
![HYDROQUINIDINE](/CAS/GIF/1435-55-8.gif)
1435-55-8
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Yield: 87%
Reaction Conditions:
Stage #1:hydroquinidine with di-isopropyl azodicarboxylate;diphenyl phosphoryl azide;triphenylphosphine in tetrahydrofuran at 0 - 50; for 16 h;
Stage #2: with water in tetrahydrofuran at 20; for 3 h;
References:
Oliva, Cristina G.;Silva, Artur M. S.;Resende, Diana I. S. P.;Paz, Filipe A. A.;Cavaleiro, Jose A. S. [European Journal of Organic Chemistry,2010,# 18,p. 3449 - 3458] Location in patent:experimental part
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trihydrochloride](/CAS/20180808/GIF/287979-82-2.gif)
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![9-AMino(9-deoxy)epi-diquinidine trihydrochloride](/CAS/20200515/GIF/522600-31-3.gif)
522600-31-3
11 suppliers
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