ChemicalBook CAS DataBase List 9-BBN TRIFLATE

9-BBN TRIFLATE synthesis

2synthesis methods

Product Name:9-BBN TRIFLATE
CAS Number:62731-43-5
Molecular formula:C9H14BF3O3S
Molecular Weight:270.07

Equimolar amounts of 9-Borabicyclo[3.3.1]nonane and Trifluoromethanesulfonic Acid are mixed in hexane and stirred at 20 °C for 24 h after which time 9-BBN TRIFLATE is isolated by vacuum distillation.

1493-13-6 Synthesis

1493-13-6
631 suppliers
$12.00/5g

280-64-8
155 suppliers
$45.00/50ml

62731-43-5
38 suppliers
$277.00/100ml

Yield:62731-43-5 85%

Reaction Conditions:

in hexane;trifluoromethanesulfonic acid addn. to 9-borabicyclo<3,1,1>nonane in hexane under Ar, stirring overnight, all at 25°C in the presence ofoxygen or air; concn., vac. distn. under Ar, IR anal.;

References:

Inoue, Tan;Mukaiyama, Teruaki [Bulletin of the Chemical Society of Japan,1980,vol. 53,# 1,p. 174 - 178]

21205-91-4 Synthesis

21205-91-4
112 suppliers
$50.00/1g

1493-13-6 Synthesis

1493-13-6
631 suppliers
$12.00/5g

62731-43-5
38 suppliers
$277.00/100ml

References

9-BBN TRIFLATE Related Search:

9-BROMO-9-BORABICYCLO[3.3.1]NONANE BETA-BENZYL-9-BBN DIBUTYLBORON TRIFLUOROMETHANESULFONATE Trifluoromethanesulfonic acid