9-broMo-10-[4-(2-naphthalenyl)phenyl]Anthracene synthesis
- Product Name:9-broMo-10-[4-(2-naphthalenyl)phenyl]Anthracene
- CAS Number:866611-29-2
- Molecular formula:C30H19Br
- Molecular Weight:459.38
866611-28-1
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866611-29-2
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Yield: 99%
Reaction Conditions:
with N-Bromosuccinimide in N,N-dimethyl-formamide at 20;
Steps:
4
9-(4-Naphthalene-2-yl-phenyl)anthracene 13.25 g was dispersed in DMF (dimethylformamide) 100 ml, and a DMF solution (100 ml) of NBS (N-bromosuccinimide) 7.44 g was dropwise added thereto at room temperature. The solution was stirred at room temperature for 7 hours and then left standing for a nigh. Water 200 ml was added thereto, and the deposited crystal was filtered, sufficiently washed with ethanol and dried, whereby targeted (9-bromo-10-(4-naphthalene-2-yl-phenyl)anthracene 15.84 g was obtained (yield: 99 %).
References:
IDEMITSU KOSAN CO., LTD. EP1707550, 2006, A1 Location in patent:Page/Page column 34
1564-64-3
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866611-29-2
50 suppliers
$105.00/200mg