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ChemicalBook CAS DataBase List 9-Bromo-9-phenylfluorene
55135-66-5

9-Bromo-9-phenylfluorene synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether; hexane / 0.83 h / 0 °C / Inert atmosphere
1.2: 2.42 h / 0 - 24 °C / Inert atmosphere
2.1: hydrogen bromide / toluene; water / 24 h / 20 - 25 °C / Inert atmosphere

References:

Jamison;Lubell;Dener;Krisché;Rapoport [Organic Syntheses,1993,vol. 71,p. 220 - 220]

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