9-Iodo-1-nonanol synthesis
- Product Name:9-Iodo-1-nonanol
- CAS Number:76334-30-0
- Molecular formula:C9H19IO
- Molecular Weight:270.15
3937-56-2
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Yield:76334-30-0 93%
Reaction Conditions:
with iodine in acetonitrile at 120; for 0.0666667 h;Microwave irradiation;chemoselective reaction;
Steps:
4. 2. Typical Procedure for Iodinationof Alcohol
General procedure: To a suspension of polymer-bound triphenylphosphine (1.2 mmol) in anhydrous acetonitrile (10 mL) were added iodine (1 mmol) and 1,6-hexanediol diol (1mmol). The reaction mixture was irradiated in microwave reactor at 120 °C for 3 min. The reaction mixture was filtered over a filter paper and washed with chloroform.The filtrate was extracted with aqueous sodium thiosulfate solution and dried with anhydrous sodium sulfate.The reafter, solvent was removed under reduced pressure to obtain 6-iodohexan-1-ol (30) in 93%
References:
Das, Diparjun;Chanda, Tridib;Rokhum, Lalthazuala [Acta Chimica Slovenica,2015,vol. 62,# 4,p. 775 - 783]
55362-80-6
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