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Carbamic acid, N-[(1S,2R)-2,3-dihydro-2-[(methylsulfonyl)oxy]-1H-inden-1-yl]-, 1,1-dimethylethyl ester synthesis

2synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
825 suppliers
$13.50/25G

Carbamic acid, N-[(1S,2R)-2,3-dihydro-2-[(methylsulfonyl)oxy]-1H-inden-1-yl]-, 1,1-dimethylethyl ester

904295-56-3
2 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 20 °C
2: triethylamine / dichloromethane / 3 h / 0 - 20 °C

References:

Gardelli, Cristina;Wada, Hiroki;Ray, Asim;Caffrey, Moya;Llinas, Antonio;Shamovsky, Igor;Tholander, Joakim;Larsson, Joakim;Sivars, Ulf;Hultin, Leif;Andersson, Ulf;Sanganee, Hitesh J.;Stenvall, Kristina;Leidvik, Brith;Gedda, Karin;Jinton, Lisa;Rydén Landergren, Marie;Karabelas, Kostas [Journal of Medicinal Chemistry,2018,vol. 61,# 14,p. 5974 - 5987]