5-FLUORO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE synthesis
- Product Name:5-FLUORO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE
- CAS Number:907973-43-7
- Molecular formula:C10H12FN
- Molecular Weight:165.21
143654-62-0
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907973-43-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 0 °C
1.2: 0 - 20 °C
2.1: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Heating / reflux
3.1: hydrogen / palladium 10% on activated carbon / ethanol
References:
US2008/119496,2008,A1
911825-55-3
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348-52-7
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93742-85-9
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166251-26-9
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907973-43-7
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