N,N-diMethyl-4-((4-((triMethylsilyl)ethynyl) phenyl)ethynyl)benzenaMine synthesis

5synthesis methods

Product Name:N,N-diMethyl-4-((4-((triMethylsilyl)ethynyl) phenyl)ethynyl)benzenaMine
CAS Number:910467-59-3
Molecular formula:C21H23NSi
Molecular Weight:317.5

Benzenamine, 4-[2-(4-iodophenyl)ethynyl]-N,N-dimethyl-

924892-34-2
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1066-54-2
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N,N-diMethyl-4-((4-((triMethylsilyl)ethynyl) phenyl)ethynyl)benzenaMine

910467-59-3
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$129.00/100mg

Yield:910467-59-3 99%

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;copper(l) iodide;triethylamine in tetrahydrofuran at 25; for 0.5 h;Inert atmosphere;Sonogashira coupling;

References:

Kulhanek, Jiri;Bures, Filip;Ludwig, Miroslav [Beilstein Journal of Organic Chemistry,2009,vol. 5,art. no. 11] Location in patent:supporting information; experimental part