3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER synthesis

2synthesis methods

Product Name:3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER
CAS Number:912760-74-8
Molecular formula:C9H9BrN2O2
Molecular Weight:257.08

1072-97-5 Synthesis

1072-97-5
689 suppliers
$9.00/1g

3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER

912760-74-8
24 suppliers
$140.00/50mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C
2: [Cp*RhCl₂]2; silver hexafluoroantimonate; copper diacetate / 1,2-dichloro-ethane / 24 h / 120 °C / Schlenk technique; Inert atmosphere
3: hydrogenchloride / methanol; water / 3 h / 60 °C

References:

Zhou, Jun;Li, Bo;Hu, Fang;Shi, Bing-Feng [Organic Letters,2013,vol. 15,# 13,p. 3460 - 3463]

N-(5-bromo-pyridin-2-yl)-2,2-dimethyl-propionamide

182344-63-4
25 suppliers
$58.00/1g

912760-74-8
24 suppliers
$140.00/50mg

References

3-(2-AMINO-5-BROMO-PYRIDIN-3-YL)-ACRYLIC ACID METHYL ESTER Related Search:

ETHYL 3-(2-AMINO-5-BROMOPYRIDIN-3-YL)ACRYLATE 2-Amino-5-bromo-3-methylpyridine