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ChemicalBook CAS DataBase List BENZYL 2,3-O-ISOPROPYLIDENE-6-TRITYL-ALPHA-D-MANNOFURANOSE

BENZYL 2,3-O-ISOPROPYLIDENE-6-TRITYL-ALPHA-D-MANNOFURANOSE synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 78 percent / methyltri-n-octylammonium chloride, 10M NaOH / benzene / 30 h / Ambient temperature
2: 94 percent / 12M HCl / methanol; H2O / 7 h / Ambient temperature
3: 66 g / pyridine / 18 h / 25 °C

References:

Legler, Guenter;Juelich, Elisabeth [Carbohydrate Research,1984,vol. 128,p. 61 - 72]