ChemicalBook CAS DataBase List Pentanoic acid, 5-hydroxy-, 1,1-dimethylethyl ester

Pentanoic acid, 5-hydroxy-, 1,1-dimethylethyl ester synthesis

5synthesis methods

Product Name:Pentanoic acid, 5-hydroxy-, 1,1-dimethylethyl ester
CAS Number:91420-49-4
Molecular formula:C9H18O3
Molecular Weight:174.24

108-55-4 Synthesis

108-55-4
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Pentanoic acid, 5-hydroxy-, 1,1-dimethylethyl ester

91420-49-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: dmap; 1-hydroxy-pyrrolidine-2,5-dione; triethylamine / toluene
2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 2 h / 0 - 20 °C

References:

Gao, Yongzhi;Van Haren, Matthijs J.;Moret, Ed E.;Rood, Johannes J. M.;Sartini, Davide;Salvucci, Alessia;Emanuelli, Monica;Craveur, Pierrick;Babault, Nicolas;Jin, Jian;Martin, Nathaniel I. [Journal of Medicinal Chemistry,2019,vol. 62,# 14,p. 6597 - 6614]

56198-37-9 Synthesis