ChemicalBook CAS DataBase List 4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-6-hydroxy-2-cycloehexen-1-one

4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-6-hydroxy-2-cycloehexen-1-one synthesis

1synthesis methods

Product Name:4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-6-hydroxy-2-cycloehexen-1-one
CAS Number:915235-16-4
Molecular formula:C14H22O2
Molecular Weight:222.32

196193-23-4 Synthesis

4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-2-cyclohexen-1-one

196193-23-4
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4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-6-hydroxy-2-cycloehexen-1-one

915235-16-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi; (i-Pr)2NH / tetrahydrofuran; hexane / 1.5 h / -78 °C
1.2: tetrahydrofuran; hexane / 5 h / -78 - 0 °C
2.1: mCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 10 h / 20 °C
2.2: 4.50 g / aq. HCl / CH₂Cl₂ / 12 h / 20 °C

References:

Chavan, Subhash P.;Thakkar, Mahesh;Jogdand, Ganesh F.;Kalkote, Uttam R. [Journal of Organic Chemistry,2006,vol. 71,# 23,p. 8986 - 8988]

4-[(1R)-1,5-Dimethyl-4-hexen-1-yl]-6-hydroxy-2-cycloehexen-1-one Related Search:

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