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1H-Imidazole-1-carboxylic acid, 2-amino-4-(dimethoxymethyl)-,1,1-dimethylethyl ester synthesis

2synthesis methods
6342-56-9 Synthesis
Methylglyoxal 1,1-dimethyl acetal

6342-56-9
305 suppliers
$8.00/25g

1H-Imidazole-1-carboxylic acid, 2-amino-4-(dimethoxymethyl)-,1,1-dimethylethyl ester

917919-48-3
6 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: bromine / tetrachloromethane / 12 h / 20 °C / Inert atmosphere
2: titanium(IV) isopropylate / tetrahydrofuran / 48 h / 20 °C

References:

Wang, Jing;Hu, Xuefeng;Wang, Dongli;Xie, Cao;Lu, Weiyue;Song, Jie;Wang, Ruifeng;Gao, Chunli;Liu, Min [Organic and Biomolecular Chemistry,2018,vol. 16,# 24,p. 4464 - 4470]

3-bromo-1,1-dimethoxy-2-Propanone

75271-94-2
8 suppliers
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219511-71-4 Synthesis
BOC-GUANIDINE

219511-71-4
104 suppliers
$6.00/1g

1H-Imidazole-1-carboxylic acid, 2-amino-4-(dimethoxymethyl)-,1,1-dimethylethyl ester

917919-48-3
6 suppliers
inquiry