1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-2,2,2-trifluoroethanol synthesis
- Product Name:1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-2,2,2-trifluoroethanol
- CAS Number:923170-94-9
- Molecular formula:C10H9F3O3
- Molecular Weight:234.1719
29668-44-8
272 suppliers
$6.00/1g
81290-20-2
409 suppliers
$13.00/1g
923170-94-9
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Yield:923170-94-9 97%
Reaction Conditions:
Stage #1: 2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde;(trifluoromethyl)trimethylsilanewith potassium carbonate in N,N-dimethyl-formamide at 20; for 4 h;
Stage #2: with water in N,N-dimethyl-formamide; for 4 h;Acidic conditions;
References:
Cheng, Huicheng;Pei, Yu;Leng, Faqiang;Li, Jingya;Liang, Apeng;Zou, Dapeng;Wu, Yangjie;Wu, Yusheng [Tetrahedron Letters,2013,vol. 54,# 33,p. 4483 - 4486]
1400691-55-5
7 suppliers
$55.39/1g
29668-44-8
272 suppliers
$6.00/1g
923170-94-9
6 suppliers
inquiry
29668-44-8
272 suppliers
$6.00/1g
923170-94-9
6 suppliers
inquiry