ChemicalBook CAS DataBase List Dihydro-4-[[3-Methoxy-4-(phenylMethoxy)phenyl]Methyl]-2(3H)-furanone

Dihydro-4-[[3-Methoxy-4-(phenylMethoxy)phenyl]Methyl]-2(3H)-furanone synthesis

11synthesis methods

Product Name:Dihydro-4-[[3-Methoxy-4-(phenylMethoxy)phenyl]Methyl]-2(3H)-furanone
CAS Number:92831-74-8
Molecular formula:C19H20O4
Molecular Weight:312.36

2426-87-1 Synthesis

2426-87-1
240 suppliers
$8.00/5g

Dihydro-4-[[3-Methoxy-4-(phenylMethoxy)phenyl]Methyl]-2(3H)-furanone

92831-74-8
8 suppliers
$1320.00/250mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium methoxide / methanol / 5.5 h / Heating
1.2: 78 percent / aq. HCl / H₂O / 0 °C
2.1: 90 percent / Mg / methanol / 5.5 h / 0 °C
3.1: LiBH₄ / tetrahydrofuran / 5.5 h / Heating
3.2: 48 percent / aq. HCl / tetrahydrofuran / 15 h / 20 °C

References:

Takemoto, Masumi;Hongo, Yoko;Aoshima, Youichi;Kutney, James Peter [Heterocycles,2006,vol. 69,# 1,p. 429 - 436]