ChemicalBook CAS DataBase List 3-[(Z)-Butylidene]-7-hydroxy-1(3H)-isobenzofuranone

3-[(Z)-Butylidene]-7-hydroxy-1(3H)-isobenzofuranone synthesis

3synthesis methods

Product Name:3-[(Z)-Butylidene]-7-hydroxy-1(3H)-isobenzofuranone
CAS Number:93236-67-0
Molecular formula:C12H12O3
Molecular Weight:0

53015-08-0
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3-[(Z)-Butylidene]-7-hydroxy-1(3H)-isobenzofuranone

93236-67-0
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: tetrahydrofuran / 1 h
2: 79 percent / I₂, KI, NaHCO₃ / H₂O / Ambient temperature
3: 63 percent / sodium acetate / ethanol / 2 h / Heating
4: 77 percent / AlCl₃ / CH₂Cl₂ / 1 h / Ambient temperature

References:

Mali, R.S.;Patil, S.R. [Synthetic Communications,1990,vol. 20,# 2,p. 167 - 173]

1(3H)-Isobenzofuranone, 3-butylidene-7-methoxy-, (Z)-

128586-32-3
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93236-67-0
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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93236-67-0
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References